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It should therefore be easy to reproduce such separations with modern columns of conventional dimensions, but I found it difficult to find a better separation in the current literature. Why is this, when so many papers appear on the topic? First, fatty ass there are large numbers of papers that deal with ever more esoteric derivatization reagents fatty ass to change the sensitivity of detection, while ignoring the actual chromatography. I have very little idea of how even the main types of derivatives in common use affect the selectivity or general quality of separations. Second, fatty ass there is a large number of papers that deal with the analysis of the biologically important free fatty acid fraction in animal tissues. Again, sensitivity is often the main point of interest (often ignoring reproducibility and the effects of gradient elution on quantification), and there appears to be little discussion of the chromatographic process.
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