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Reference oil samples from email lists animal and vegetal origin may be ordered from the American Oil Chemical Society email lists which gives also analysis sheets of results. A general method was accurately described for the analysis of milk fat with details on peak quantification (Collomb M et al. Mitt Lebensm Hyg 2000, 91, 306). An automated analysis of fatty acid methyl esters using a XYZ robotic autosampler has been described (de Koning S et al., J Chromatogr A 2001, 922, 391). After preparing manually a solution of fatty acids, email lists the autosampler is used to add reagent (sodium methylate), agitate, and finally inject into the gas chromatograph. That procedure takes about 15 min before analysis of the samples. The separation of fatty acids of the palmitoleate series (n-7) from the n-6 series may be improved in using a specific capillary column coated with cyanopropyl polysiloxane as it was proposed for the study of liver fatty acids associated with fat deficiency (Wolff RL et al.,
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